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[Application]N-FMOC-DL-Leucine
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N-FMOC-DL-Leucine
COMPOUND IDENTIFICATION
| Compound Name | N-FMOC-DL-Leucine |
|---|
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name Column Size / Particle Size |
CHIRALPAK® QN-AX 150 x 4.6mm / 5µm |
|---|---|
|
Mobile Phase Composition |
methanol / acetic acid / NH4OAc = 98 / 2 / 0.5 |
|
Chromatographic Mode |
Polar Phase |
|
Flow rate (ml/min) |
1 |
Injection amount (mg) |
0.01 |
|---|---|---|---|
|
Temperature (°C) |
25 |
Pressure (MPa) |
|
|
Detection |
UV 254 nm |
Elution order |
|
|
No. |
Rt |
K’ |
|---|---|---|
|
1 |
5.21 |
1.8 |
|
2 |
7.95 |
3.27 |
|
|
Alpha Value |
Resolution |
|---|---|---|
|
1 - 2 |
1.82 |
7.43 |
N-FMOC-DL-Leucine
COMPOUND IDENTIFICATION
| Compound Name | N-FMOC-DL-Leucine |
|---|
CHROMATOGRAM
ANALYTICAL REPORT
|
Column Trade Name Column Size / Particle Size |
CHIRALPAK® QD-AX 150 x 4.6mm / 5µm |
|---|---|
|
Mobile Phase Composition |
acetonitrile / acetic acid = 97 / 3 |
|
Chromatographic Mode |
Polar Phase |
|
Flow rate (ml/min) |
1 |
Injection amount (mg) |
0.01 |
|---|---|---|---|
|
Temperature (°C) |
25 |
Pressure (MPa) |
|
|
Detection |
UV 254 nm |
Elution order |
|
|
No. |
Rt |
K’ |
|---|---|---|
|
1 |
11.04 |
5.06 |
|
2 |
14.18 |
6.78 |
|
|
Alpha Value |
Resolution |
|---|---|---|
|
1 - 2 |
1.34 |
5.87 |
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