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[Application](4R,5S/4S,5R)-1,5-Dimethyl-4-phenyl-2-imidazolidinone

관리자 | 2017.07.03 11:44 | 조회 3479

(4R,5S/4S,5R)-1,5-Dimethyl-4-phenyl-2-imidazolidinone

COMPOUND IDENTIFICATION

Compound Name (4R,5S/4S,5R)-1,5-Dimethyl-4-phenyl-2-imidazolidinone

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IA-3

150 x 4.6mm / 3µm

Mobile Phase Composition

dichloromethane / ethanol = 98 / 2

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

0.02

Temperature (°C)

25

Pressure (MPa)

 

Detection

UV 254 nm

Elution order

 

No.

Rt

K’

1

5.36

2.15

2

7.09

3.17

 

Alpha Value

Resolution

1 - 2

1.47

8.32








(4R,5S/4S,5R)-1,5-Dimethyl-4-phenyl-2-imidazolidinone

COMPOUND IDENTIFICATION

Compound Name (4R,5S/4S,5R)-1,5-Dimethyl-4-phenyl-2-imidazolidinone

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IA-3

150 x 4.6mm / 3µm

Mobile Phase Composition

n-hexane / 2-propanol = 80 / 20

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

0.0025

Temperature (°C)

25

Pressure (MPa)

 

Detection

UV 210 nm

Elution order

 

No.

Rt

K’

1

3.86

1.27

2

4.85

1.85

 

Alpha Value

Resolution

1 - 2

1.46

6.43








(4R,5S/4S,5R)-1,5-Dimethyl-4-phenyl-2-imidazolidinone

COMPOUND IDENTIFICATION

Compound Name (4R,5S/4S,5R)-1,5-Dimethyl-4-phenyl-2-imidazolidinone

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® IC-3

150 x 4.6mm / 3µm

Mobile Phase Composition

dichloromethane / ethanol = 98 / 2

Chromatographic Mode

Normal Phase
Primary screening solvent (Immobilised CSP)

Flow rate (ml/min)

1

Injection amount (mg)

0.02

Temperature (°C)

25

Pressure (MPa)

 

Detection

UV 230 nm

Elution order

 

No.

Rt

K’

1

10.35

5.05

2

12.39

6.25

 

Alpha Value

Resolution

1 - 2

1.24

4.52










씨티케이는 DAICEL 키랄 컬럼 국내 독점판매처입니다.

제품에 대한 문의는 아래의 연락처 참조 부탁드립니다.

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