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[Application]N-3,5-DNB-DL-Leucine

관리자 | 2017.07.26 09:48 | 조회 3108

N-3,5-DNB-DL-Leucine

COMPOUND IDENTIFICATION

Compound Name N-3,5-DNB-DL-Leucine

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® AGP

100 x 4mm / 5µm

Mobile Phase Composition

10mM NH4OAc aq. pH4.5 / acetonitrile = 90 / 10

Chromatographic Mode

Reverse Phase

Flow rate (ml/min)

0.9

Injection amount (mg)

0.0005

Temperature (°C)

20

Pressure (MPa)

 

Detection

UV 225 nm

Elution order

 

No.

Rt

K’

1

5.56

4.48

2

6.81

5.71

 

Alpha Value

Resolution

1 - 2

1.28

1.89









N-3,5-DNB-DL-Leucine

COMPOUND IDENTIFICATION

Compound Name N-3,5-DNB-DL-Leucine

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® HSA

100 x 4mm / 5µm

Mobile Phase Composition

10mM NH4OAc aq. (+5mM heptafluorobutyric acid) pH7.0 / 2-propanol = 85 / 15

Chromatographic Mode

Reverse Phase

Flow rate (ml/min)

0.9

Injection amount (mg)

0.0005

Temperature (°C)

20

Pressure (MPa)

 

Detection

UV 225 nm

Elution order

 

No.

Rt

K’

1

6.96

5.46

2

10.28

8.54

 

Alpha Value

Resolution

1 - 2

1.56

2.08









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