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[Application]N-CBZ-DL-Leucine

관리자 | 2017.07.26 09:49 | 조회 2400

N-benzoyl-DL-Leucine

COMPOUND IDENTIFICATION

Compound Name N-benzoyl-DL-Leucine

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® HSA

100 x 4mm / 5µm

Mobile Phase Composition

10mM NH4OAc aq. (+10mM heptafluorobutyric acid aq.) pH7.0 / 2-propanol = 90 / 10

Chromatographic Mode

Reverse Phase

Flow rate (ml/min)

0.9

Injection amount (mg)

0.0025

Temperature (°C)

20

Pressure (MPa)

 

Detection

UV 225 nm

Elution order

 

No.

Rt

K’

1

2.19

1.03

2

3.39

2.14

 

Alpha Value

Resolution

1 - 2

2.06

2.53








N-CBZ-DL-Leucine

COMPOUND IDENTIFICATION

Compound Name N-CBZ-DL-Leucine

CHROMATOGRAM

ANALYTICAL REPORT

Column Trade Name

Column Size / Particle Size

CHIRALPAK® HSA

100 x 4mm / 5µm

Mobile Phase Composition

10mM NH4OAc aq. (+2mM octanoic acid aq.) pH7.0 / 2-propanol = 85 / 15

Chromatographic Mode

Reverse Phase

Flow rate (ml/min)

0.9

Injection amount (mg)

0.0025

Temperature (°C)

20

Pressure (MPa)

 

Detection

UV 210 nm

Elution order

 

No.

Rt

K’

1

4.32

3.01

2

9.1

7.44

 

Alpha Value

Resolution

1 - 2

2.47

2.64








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