Application data

분리 조건 검토 예

2L-ChiralTLC IA
Warfarin Sodium N-CBZ-DL-Valine Flavanone
Plate size: 10mm×100mm
Solvent:n-Hex./IPA/TFA=50/50/0.1(v/v/v)
Sample conc.: 50,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm
Plate size: 10mm×100mm
Solvent:n-Hex./IPA/TFA=70/30/0.1(v/v/v)
Sample conc.: 100,000ppm in Eluent
Inj. : 1μL.
Detect:Phosphomolybdic acid
Plate size: 10mm×100mm
Solvent:n-Hex./EtOAc=90/10(v/v)
Sample conc.: 5,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm


2L-ChiralTLC IC
4-Benzoyloxy-2-azetidinone Pindolol 1,5-dihydroxy-1,2,3,4-tetrahydronaphthalene
Plate size: 10mm×100mm
Solvent:n-Hex./IPA/TFA=50/50/0.1(v/v/v)
Sample conc.: 50,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm
Plate size: 10mm×100mm
Solvent:n-Hex./IPA/TFA=70/30/0.1(v/v/v)
Sample conc.: 100,000ppm in Eluent
Inj. : 1μL.
Detect:Phosphomolybdic acid
Plate size: 10mm×100mm
Solvent:n-Hex./EtOAc=90/10(v/v)
Sample conc.: 5,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm


2L-ChiralTLC ID
Flavanone Aminoglutethimide
Plate size: 10mm×100mm
Solvent:MeOH=100(v)
Sample conc.: 5,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm
Plate size: 10mm×100mm
Solvent:EtOAc/DEA=100/0.1(v/v)
Sample conc.: 50,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm


2L-ChiralTLC IF
Tröger's base Furoin Methyclothiazide
Plate size: 10mm×100mm
Solvent:MeOH=100(v)
Sample conc.: 10,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm
Plate size: 10mm×100mm
Solvent:n-Hex./EtOH/MeOH=30/40/40(v/v/v)
Sample conc.: 50,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm
Plate size: 10mm×100mm
Solvent:n-Hex./EtOH/DEA=50/50/0.1(v/v)
Sample conc.: 10,000ppm in Eluent
Inj. : 1μL.
Detect:UV254nm