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Application data
분리 조건 검토 예
2L-ChiralTLC IA
Warfarin Sodium | N-CBZ-DL-Valine | Flavanone |
---|---|---|
Plate size: 10mm×100mm Solvent:n-Hex./IPA/TFA=50/50/0.1(v/v/v) Sample conc.: 50,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |
Plate size: 10mm×100mm Solvent:n-Hex./IPA/TFA=70/30/0.1(v/v/v) Sample conc.: 100,000ppm in Eluent Inj. : 1μL. Detect:Phosphomolybdic acid |
Plate size: 10mm×100mm Solvent:n-Hex./EtOAc=90/10(v/v) Sample conc.: 5,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |
2L-ChiralTLC IC
4-Benzoyloxy-2-azetidinone | Pindolol | 1,5-dihydroxy-1,2,3,4-tetrahydronaphthalene |
---|---|---|
Plate size: 10mm×100mm Solvent:n-Hex./IPA/TFA=50/50/0.1(v/v/v) Sample conc.: 50,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |
Plate size: 10mm×100mm Solvent:n-Hex./IPA/TFA=70/30/0.1(v/v/v) Sample conc.: 100,000ppm in Eluent Inj. : 1μL. Detect:Phosphomolybdic acid |
Plate size: 10mm×100mm Solvent:n-Hex./EtOAc=90/10(v/v) Sample conc.: 5,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |
2L-ChiralTLC ID
Flavanone | Aminoglutethimide |
---|---|
Plate size: 10mm×100mm Solvent:MeOH=100(v) Sample conc.: 5,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |
Plate size: 10mm×100mm Solvent:EtOAc/DEA=100/0.1(v/v) Sample conc.: 50,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |
2L-ChiralTLC IF
Tröger's base | Furoin | Methyclothiazide |
---|---|---|
Plate size: 10mm×100mm Solvent:MeOH=100(v) Sample conc.: 10,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |
Plate size: 10mm×100mm Solvent:n-Hex./EtOH/MeOH=30/40/40(v/v/v) Sample conc.: 50,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |
Plate size: 10mm×100mm Solvent:n-Hex./EtOH/DEA=50/50/0.1(v/v) Sample conc.: 10,000ppm in Eluent Inj. : 1μL. Detect:UV254nm |